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Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods with acceptable restrictions
Remarks:
Laser diffraction is the well experienced standard procedure for pigments to determine particle size distribution of the substance as it is manufactured and delivered.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2007
Report date:
2007

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Principles of method if other than guideline:
Laser diffraction particle sizing
Type of method:
Laser scattering/diffraction
Type of distribution:
volumetric distribution

Test material

Constituent 1
Chemical structure
Reference substance name:
2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[3-oxo-N-phenylbutyramide]
EC Number:
228-787-8
EC Name:
2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[3-oxo-N-phenylbutyramide]
Cas Number:
6358-85-6
Molecular formula:
C32H26Cl2N6O4
IUPAC Name:
2-[2-(3,3'-dichloro-4'-{2-[2-oxo-1-(phenylcarbamoyl)propyl]diazen-1-yl}-[1,1'-biphenyl]-4-yl)diazen-1-yl]-3-oxo-N-phenylbutanamide
Test material form:
solid: nanoform

Results and discussion

Particle sizeopen allclose all
Percentile:
D50
Mean:
3.37 µm
St. dev.:
0.44
Percentile:
D10
Mean:
0.54 µm
St. dev.:
0.05
Percentile:
D90
Mean:
145.6 µm
St. dev.:
41

Any other information on results incl. tables

Given standard deviation is based on the general experience with pigments and the method. The estimated values are typical standard deviations:

D10: 4 % of D10 (minimum value 0.05 µm)

D50: 13 % of D50 (minimum value 0.1 µm)

D90: 29 % of D90 - D50

Applicant's summary and conclusion