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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
25 July 2017 - 27 November 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
Qualifier:
according to guideline
Guideline:
ASTM D93 (Standard test methods for flash point by pensky-martens closed cup tester)
Deviations:
no
Qualifier:
according to guideline
Guideline:
ISO 2719 (Determination of flash point - Pensky-Martens closed cup method)
Deviations:
no
Qualifier:
according to guideline
Guideline:
ISO 3679 (Determination of flash point - Rapid equilibrium closed cup method)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: ASTM D7094: “Standard Test Method for Flash Point by Modified Continuously Closed Cup (MCCCFP) Tester”
Qualifier:
according to guideline
Guideline:
other: UN no. ST/SG/AC.10/11/Rev.6 “Non-Viscous Flammable Liquids”
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: United Nations (UN), UN no. ST/SG/AC.10/11/Rev.6
Version / remarks:
United Nations (UN), UN no. ST/SG/AC.10/11/Rev.6: Recommendations on the Transport of
Dangerous Goods, Part III: Classification Procedures, Test Methods and Criteria Relating to
Class 2, Class 3, Class 4, Division 5.1, Class 8 and Class 9, Paragraph 32.4.1: “Non-Viscous
Flammable Liquids”, 2015.
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
closed cup
Flash point apparatus:
other: Eraflash flash-point tester

Test material

Constituent 1
Chemical structure
Reference substance name:
Diethyl ethoxymethylenemalonate
EC Number:
201-725-7
EC Name:
Diethyl ethoxymethylenemalonate
Cas Number:
87-13-8
Molecular formula:
C10H16O5
IUPAC Name:
diethyl ethoxymethylenemalonate
Test material form:
liquid
Specific details on test material used for the study:
- Batch n°: JC170405
- Analytical purity: 99.5%
- Expiration date: 12 April 2018
- Storage condition: at room temperature

Results and discussion

Flash point
Key result
Flash point:
142 °C
Atm. press.:
1 013.25 hPa

Any other information on results incl. tables

Preliminary test

The estimated flash-point of the test item was 139°C.

Main study

The difference between the results obtained with the two tests was ≤ 6°C. From this, it was concluded that the flash-point of the test item is the lowest flash-point obtained.

 Test Flash-point

°C

 Lowest flash-point  

°C

 1 142  142 
 2 144  

Applicant's summary and conclusion

Interpretation of results:
GHS criteria not met
Conclusions:
The closed cup method was applied for the determination of the flash-point of JNJ-39005525-AAA (EMME).
The flash-point of the test item was 142°C.