Registration Dossier

Administrative data

Endpoint:
auto-flammability
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing was conducted between 15 September 2010 and 24 September 2010.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010

Materials and methods

Test guideline
Qualifier:
according to
Guideline:
other: Testing was conducted using a procedure designed to be compatible with Method A15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
Deviations:
no
GLP compliance:
yes (incl. certificate)

Test material

Reference
Name:
Unnamed
Type:
Constituent
Details on test material:
Sponsor's identification: X-3383
Description : pale yellow viscous liquid
Batch number : not supplied
Label : INVENTORY NO: X-3383
Date received : 10 August 2010
Expiry date : 06 August 2016
Storage conditions: room temperature in the dark

Results and discussion

Auto-ignition temperature (liquids / gases)
Auto-ignition temperature:
262 °C
Atm. press.:
> 100.24 - 101.72 kPa
Remarks on result:
other:
Relative self-ignition temperature (solids)
Relative self-ignition temperature:
262 °C
Remarks on result:
other:
Remarks:
at atm. press. of >100.24 - 101.72 kPa

Any other information on results incl. tables

Results

Test Temperature (ºC)

Test Volume (µl)

Ignition Delay (s)

Observations

200 (clean flask)

70

>300

No ignition, grey fumes emitted.

250

70

>300

No ignition, grey fumes emitted.

300 (clean flask)

70

5

Orange flame, grey fumes emitted.

280

70

>300

No ignition, grey fumes emitted.

290

70

10

Orange flame, grey fumes emitted.

284

70

15

Orange flame, grey fumes emitted.

282 (clean flask)

70

23

Orange flame, grey fumes emitted.

280 (clean flask)

70

29

Orange flame, grey fumes emitted.

276 (clean flask)

70

31

Orange flame, grey fumes emitted.

272 (clean flask)

70

>300

No ignition, grey fumes emitted.

274 (clean flask)

70

>300

No ignition, grey fumes emitted.

274 (clean flask)

200

38

Orange flame, grey fumes emitted.

272 (clean flask)

200

43

Orange flame, grey fumes emitted.

270 (clean flask)

200

46

Orange flame, grey fumes emitted.

266 (clean flask)

200

54

Orange flame, grey fumes emitted.

262 (clean flask)

200

>300

No ignition, grey fumes emitted.

264 (clean flask)

200

42

Orange flame, grey fumes emitted.

262 (clean flask)

400

>300

No ignition, grey fumes emitted.

262 (clean flask)

600

>300

No ignition, grey fumes emitted.

262 (clean flask)

800

214

Orange flame, grey fumes emitted.

260 (clean flask)

800

>300

No ignition, grey fumes emitted.

260 (clean flask)

1000

>300

No ignition, grey fumes emitted.

260 (clean flask)

1200

>300

No ignition, grey fumes emitted.

260 (clean flask)

1400

>300

No ignition, grey fumes emitted.

260 (clean flask)

1600

>300

No ignition, grey fumes emitted.

Room temperature:  20°C
Atmospheric pressure: 100.24 to 101.72 kPa

Applicant's summary and conclusion

Conclusions:
The test item has been determined to have an auto-ignition temperature of 262 ± 5°C.
Executive summary:

INTRODUCTION

Hazardous physico-chemical properties of the test item have been determined.

Methods employed are designed to be compatible with those specified in Commission Regulation (EC) No 440/2008 of 30 May 2008, Part A: Methods for the determination of physico-chemical properties and the current OECD Guidelines for Testing of Chemicals.

Method

The auto-ignition temperature was determined by heating aliquots of the test item in a flask and observing for any ignition. Testing was conducted using a procedure designed to be compatible with Method A15 Auto-Ignition Temperature (Liquids and Gases) ofCommissionRegulation (EC) No 440/2008 of 30 May 2008.

Conclusion

The test item has been determined to have an auto-ignition temperature of 262 ± 5°C.