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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
from 1989, october 16th to 1989, october 18th
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP study performed according to the Test Guidelines described in the EEC Directive 84/449/EEC.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1989
Report date:
1989

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes
Type of method:
capillary method

Test material

Constituent 1
Chemical structure
Reference substance name:
3',5'-dichloro-4'-ethyl-2'-hydroxypalmitanilide
EC Number:
406-200-8
EC Name:
3',5'-dichloro-4'-ethyl-2'-hydroxypalmitanilide
Cas Number:
117827-06-2
Molecular formula:
C24H39Cl2NO2
IUPAC Name:
N-(3,5-dichloro-4-ethyl-2-hydroxyphenyl)hexadecanamide
Details on test material:
Identification UC—136
Description White powder
Purity 98.5%
Storage conditions At room temperature in the dark in a tightly sealed container.
Stability of the test substance : Stable for one year maximal under storage conditions.
Safety precautions Gloves and goggies were used to assure personnel health and safety.
The test was perf’ormed in a fume cupboard.

Results and discussion

Melting / freezing point
Melting / freezing pt.:
>= 350.5 - <= 351.8 K
Atm. press.:
ca. 1 atm
Decomposition:
no
Sublimation:
no

Applicant's summary and conclusion

Conclusions:
The melting point/melting range of’ UC—136 was determined using the
capillary method. The temperature at the beginning and at the final stage
of the melting process of’ UC—136 was determined to be 350.5 K (77.3°C) and
351.8 K (78.6°C), respectively. During the melting process, the test
substance changed from a white, somewhat slightly—pink coloured solid into
a dear, slightly—pink coloured liquid.