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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From 22 June 2003 to 3 July 2003
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: ASTM Test Method D97-87
Deviations:
no
Principles of method if other than guideline:
Substance solidified without crystallisation at approximately -4.5°C and so pour point test was implemented instead of freezing point
GLP compliance:
yes (incl. QA statement)
Type of method:
pour point
Key result
Melting / freezing pt.:
0 °C
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Pour point
Conclusions:
The lowest temperature at which the test substance was still observed to flow was 0 °C.
Executive summary:

The registered substance solidified without crystallisation at a temperature of -4.5 °C and so a pour point test was conducted instead according to ASTM Test Method D97 -87. The pour point is defined as the lowest temperature at which the substance will still flow. The pour point of the resgistered substance was identified as 0 °C.

Description of key information

The study was performed on the registered substance. The pour point was reported as 0 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
0 °C

Additional information

The study was performed on the registered substance. A preliminary freezing temperature study indicated that the substance was solidifying around -4.5 °C. As a result, it was decided to perform an evaluation of the pour point according to ASTM Test Method D97-87. The pour point of the registered substance was determined to be 0 °C.