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Administrative data

Endpoint:
auto-flammability
Type of information:
experimental study
Adequacy of study:
key study
Study period:
06 October 2009 to 07 October 2009
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
Date of GLP inspection: 19-08-2008 Date of Signature on GLP certificate: 04-03-2009

Test material

Reference
Name:
Unnamed
Type:
Constituent
Type:
Constituent
Details on test material:
- Name of test material (as cited in study report): MTDID 8191
- Substance type: UVCB material
- Physical state: Yellowish viscous liquid
- Concentration of oligomers: ≥99.0%
- Purity test date: 21 January 2010
- Lot/batch no.: MK 12/048
- Expiration date of the lot/batch: 27-Jan-2010
- Stability under test conditions: Not reported
- Storage condition of test material: In the refrigerator at about 5 °C

Results and discussion

Auto-ignition temperature (liquids / gases)
Auto-ignition temperature:
> 400 °C
Atm. press.:
100.13 - 101.18 kPa
Remarks on result:
other:

Any other information on results incl. tables

Table, Conditions and observations during auto-ignition tests
Test Temperature (°C) Test Volume (µL) Ignition Delay (s) Observations
50 (clean flask) 70 >300 No ignition.
100 70 >300 No ignition.
150 70 >300 No ignition.
200 70 >300 No ignition, grey fumes emitted.
250 70 >300 No ignition, grey fumes emitted.
300 (clean flask) 70 >300 No ignition, grey fumes emitted.
350 70 >300 No ignition, grey fumes emitted.
400 (clean flask) 70 >300 No ignition, grey fumes emitted.
400 (clean flask) 200 >300 No ignition, grey fumes emitted.
400 (clean flask) 400 >300 No ignition, grey fumes emitted.
400 (clean flask) 600 >300 No ignition, grey fumes emitted.
400 (clean flask) 800 >300 No ignition, grey fumes emitted.
400 (clean flask) 1000 >300 No ignition, grey fumes emitted.

Applicant's summary and conclusion

Conclusions:
The test material has been determined not to have an auto-ignition temperature below 400°C.
Executive summary:

The auto-ignition temperature of the test material was evaluated using Method A15

Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.

The test material has been determined not to have an auto-ignition temperature below 400°C.