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Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
28 March - 18 April, 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
Version / remarks:
2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)

Test material

Constituent 1
Reference substance name:
Thiocyanic acid, (1,3,8,10-tetrahydro-1,3,8,10-tetraoxoanthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-2,9-diyl)di-3,1-phenylene ester, reaction products with sodium sulfide (Na2(Sx))
EC Number:
271-559-8
EC Name:
Thiocyanic acid, (1,3,8,10-tetrahydro-1,3,8,10-tetraoxoanthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-2,9-diyl)di-3,1-phenylene ester, reaction products with sodium sulfide (Na2(Sx))
Cas Number:
68585-53-5
Molecular formula:
not applicable
IUPAC Name:
Reaction product of thiocyanic acid, (1,3,8,10-tetrahydro-1,3,8,10-tetraoxoanthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-2,9-diyl)di-3,1-phenylene ester with sodium sulfide
Test material form:
solid: particulate/powder
Details on test material:
Test item: Leuco Sulfur Red 14
Appearance: light red solid
CAS No: 68585-53-5
EC No: 271-559-8
Specific details on test material used for the study:
Expiry date 06 March 2020
Storage room temperature

Results and discussion

Relative self-ignition temperature (solids)
Key result
Relative self-ignition temperature:
398 °C

Any other information on results incl. tables

Results of the three consecutive tests were 397.5 °C, 398.7 °C and 400.9 °C. The relative self-ignition temperature of Leuco Sulfur Red 14 was found to be 398 °C.

Applicant's summary and conclusion

Conclusions:
The relative self-ignition temperature of Leuco Sulfur Red 14 was determined to be 398 °C
Executive summary:

The objective of the study was to evaluate the relative self-ignition temperature of Leuco Sulfur Red 14.

A certain volume of the test item under the assay was placed into an oven at ambient temperature; the temperature/time curve was recorded while the temperature of the oven was increased up to 400 °C, at a rate of approximately 0.5 °C/min. For the purpose of this test, the temperature of the oven at which the sample temperature reachesby self-heating is called the self-ignition temperature.Three replicate tests were performed. The relative self-ignition temperature ofLeuco Sulfur Red 14was determined to be 398 °C.