(3S,5S)-5-[(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl]-3-(propan-2-yl)oxolan-2-one

Boiling point

Administrative data

Endpoint:

boiling point

Type of information:

experimental study

Adequacy of study:

key study

Study period:

29.4.2005

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

other: GLP-Guideline study

Data source

Reference

Reference Type:

study report

Title:

Unnamed

Year:

2005

Report date:

2005

Materials and methods

Test guideline

Qualifier:

according to guideline

Guideline:

EU Method A.2 (Boiling Temperature)

Deviations:

no

GLP compliance:

yes

Type of method:

differential scanning calorimetry

Test material

Test material information

Constituent 1

Reference substance name:

(3S,5S)-5-[(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl]-3-(propan-2-yl)oxolan-2-one

EC Number:

608-748-5

Cas Number:

324763-46-4

Molecular formula:

C25 H39 N3 O5

IUPAC Name:

(3S,5S)-5-[(1S,3S)-1-azido-3-{[4-methoxy-3-(3-methoxypropoxy)phenyl]methyl}-4-methylpentyl]-3-(propan-2-yl)oxolan-2-one

Results and discussion

Boiling point

Decomposition:

yes

Decomp. temp.:

161 °C

Any other information on results incl. tables

The melting temperature of test substance was determined to be 59°C (332 K). Probably because of a small amount of impurities, the melting process started already at 52°C - 54°C (325 K - 327 K). Reaction or decomposition of the test substance was observed above 161°C - 163°C (434 K - 436 K). Boiling of the test substance was not observed below the temperature at which reaction or decomposition started.